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RAS Chemistry & Material ScienceЖурнал физической химии Russian Journal of Physical Chemistry

  • ISSN (Print) 0044-4537
  • ISSN (Online) 3034-5537

Mechanosynthesis of Sulfur-Containing Silver Halide Nanocomposites in a Dimethyl Sulfoxide Medium

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PII
10.31857/S0044453723100254-1
DOI
10.31857/S0044453723100254
Publication type
Status
Published
Authors
F. Kh. Urakaev
  • Affiliation:
    Sobolev Institute of Geology and Mineralogy, Siberian Branch, Russian Academy of Sciences
    Al-Farabi Kazakh National University
M. M. Burkitbayev
  • Affiliation: Al-Farabi Kazakh National University
Volume/ Edition
Volume 97 / Issue number 10
Pages
1471-1480
Abstract
Transformations in the S–AgNO3–NH4X–NH4NO3 (X = Cl, Br, I) system show that nanoparticles and nanocomposites with a controlled size of particles and content of components can be synthesized via mechanical treatment and adding small amounts of a liquid in which the precursors are soluble. Nanoparticles form in a dimethyl sulfoxide (DMSO) medium through conventional (continuous dissolution–crystallization) or reactive means (continuous dissolution of precursors and their reacting with subsequent crystallization of the target product), rather than by direct mechanical activation. The first version is used for synthesizing sulfur nanoparticles (nanosulfur); the second, for synthesizing silver halides. Sulfur-containing S/AgX nanocomposites with a controlled content of sulfur are synthesized mechanochemically. A predetermined content of nanosulfur in the nanocomposites is obtained via the dissolution–crystallization (recrystallization) of sulfur in DMSO inside a mechanochemical reactor. The proposed technical solution allows the synthesis of S/AgX nanocomposites through processing AgNO3, NH4X, and NH4NO3 (diluent) precursors, commercial sulfur, and small amounts of DMSO in planetary ball mills with different fittings. The water-soluble components of the product of mechanosynthesis are readily washed off.
Keywords
механосинтез сера галогениды серебра диметилсульфоксид механохимическая перекристаллизация наночастицы нанокомпозиты
Date of publication
12.09.2025
Year of publication
2025
Number of purchasers
0
Views
10

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