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RAS Chemistry & Material ScienceЖурнал физической химии Russian Journal of Physical Chemistry

  • ISSN (Print) 0044-4537
  • ISSN (Online) 3034-5537

EVOLUTION OF MACROSCOPIC PROPERTIES OF THE SYSTEM DURING SOL-GEL SYNTHESIS OF LEAD ZIRCONATE TITANATE CERAMICS PRECURSOR

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PII
S3034553725080065-1
DOI
10.7868/S3034553725080065
Publication type
Article
Status
Published
Authors
N.D. Paramonova
  • Affiliation:
    Joint Stock Company "Research Institute of Graphite-Based Structural Materials "NIlgraphite" (JSC NIlgraphite)
    FGBOU VO "Mendeleev Russian Chemical Technology University" (D. I. Mendeleev RCTU)
E.A. Danilov
  • Affiliation: Joint Stock Company "Research Institute of Graphite-Based Structural Materials "NIlgraphite" (JSC NIlgraphite)
M.A. Vartanian
  • Affiliation: FGBOU VO "Mendeleev Russian Chemical Technology University" (D. I. Mendeleev RCTU)
Volume/ Edition
Volume 99 / Issue number 8
Pages
1170-1178
Abstract
The influence of the amount of hydrolyzing agent on the kinetics of hydrolysis of lead zirconate-titanate precursor solution is considered from the point of view of the rate of change of hydrodynamic diameters of primary particles of the sol formed at the first stage, evolution of particle size distributions, rheological and optical properties of the colloidal systems. It is shown that changing the ratio of hydrolyzing agent: organometallic compounds is an effective controlling factor at the early stage of sol-gel-synthesis of piezoceramics of lead zirconate-titanate system and allows to obtain gel with controlled speed and necessary particle sizes.
Keywords
пьезокерамика цирконат-титанат свинца золь–гель оптическая плотность вязкость динамическое светорассеяние
Date of publication
01.08.2025
Year of publication
2025
Number of purchasers
0
Views
19

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